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NEW! forced air method--CDS Chlorine dioxide solution (MMS)
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Re: NEW! forced air method--CDS Chlorine dioxide solution (MMS) 06 Dec 2011 19:06 #8915

  • polo
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I run across a .pdf pamphlet that describes how the chemical industry recommends making a CD solution at

www.docstoc.com/docs/38958828/Laboratory-Preparations-Of-Chlorine-Dioxide-Solutions

It describes an interesting setup not too unlike what is being done here.





What I find interesting is that there is a "gas scrubbing tower" in between the reaction flask and the CDS bottle in its ice bath. Supposedly in this scrubbing tower is simply a sodium chlorite solution. Any one have an idea what this does?

doug
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Re: NEW! forced air method--CDS Chlorine dioxide solution (MMS) 06 Dec 2011 20:20 #8918

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Hello Polo.
The scrubbing tower works as a filter.
The air flow may transport unwanted liquid particles that are kept in the scrubbing tower in such a way that the final solution is not polluted.
Alanti

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Re: NEW! forced air method--CDS Chlorine dioxide solution (MMS) 06 Dec 2011 20:29 #8919

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Okkkkkk, so tell me why we shouldn't be some what worried about it in our own more primitive setup that doesnt have a scrubbing tower?

Also, can you be more specific, exactly what are these "unwanted liquid particles" they are trying to filter out of the same type of acidified Sodium Chlorite solution that we use and how does simply another batch of the same sodium chlorite solution do that?

thanks,

doug

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Re: NEW! forced air method--CDS Chlorine dioxide solution (MMS) 06 Dec 2011 20:36 #8920

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Doug,


The unwanted particles come from the liquid in the reaction chamber.
Without airflow such particles are really minimal.
In any case if the ClO2 solution is not intended for IV infusions, there is nothing to worry about.
Regards.
Alanti

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Re: NEW! forced air method--CDS Chlorine dioxide solution (MMS) 06 Dec 2011 21:14 #8923

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I just run across this and is this the answer?

Chlorite is the major inorganic by-product of the reaction of chlorine dioxide in water. Usually, the amount of chlorite formed will be 40-60% of the amount of chlorine dioxide which has reacted. For example, if 1.00 ppm of chlorine dioxide is added to water and 10 minutes later, 0.60 ppm remains as a residual, 0.40 ppm has therefore reacted. We can expect the chlorite to be 0.16 - 0.24 ppm


So would the scrub tower remove this Chlorite by-product?

doug
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MMS (Master Mineral Solution) is Sodium Chlorite 28% (22.4% Sodium Chlorite, 5.6% Inert Salts and the remainder water) plus an acidic activator (usually 50% Citric Acid or 4% Hydrochloric Acid) when combined produces Chlorine Dioxide.

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